Step 1: Understanding the Carius Method
The Carius method is used to determine the percentage composition of halogens, sulphur, and phosphorus in an organic compound.
Step 2: How the Carius Method Works
- The organic compound is oxidized using fuming nitric acid in a Carius tube.
- Sulphur is converted into sulphuric acid, which is then precipitated as barium sulphate.
- The mass of precipitate helps determine the percentage of sulphur.
Conclusion
Thus, the correct answer is:
\[
\text{Sulphur}
\]